HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-Butylamine → HCID 20362847, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-Butylamine | HCID 6385 | — |
| Reactant | HCID 20362850 | HCID 20362850 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 20362847 | HCID 20362847 | — |
Reaction Steps
A solution of 1.13 g of 3-chloro-4-(2,3-epoxypropoxy)indole (prepared in manner analogous to the preparation of the starting material in Example 1, m.p. 107°-110°) and 2.2 g tert.butylamine in 15 ml of dioxan are boiled under reflux for 5 hours, evaporated to dryness and the title compound recrystallised from ether/petroleum ether. M.p. 95°-97°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04080463 |
| Source dataset | uspto-grants-1978_03 |
| ORD ID | ord-9545d257f42549b28e912e5e2d8979e8 |
| Source note | uspto-grants-1978_03 |