Ethanolamine → HCID 178506611, compound

Participants

Reaction Conditions

Reaction Steps

5.0 gm (0.0129 mol) of 2-methylmercapto-4-(2',6'-dichloro-phenyl)-2-imidazoline hydroiodide and 7.9 gm (0.13 mol) of ethanolamine were dissolved in 30 ml of ethanol, and the solution was heated in an autoclave for 3 hours at 130° C. Thereafter, the reaction solution was cooled and then admixed with ether, and the crystals precipitated thereby were collected, washed with acetone and recrystallized from ethanol/ether, yielding 1.5 gm (29% of theory) of the pure compound of the formula ##STR14##

Provenance & Evidence