3-Aminophenol → HCID 70620130, compound

HRID 1679488Notes

Reaction equation

HRID 1679488 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]([OH:8])[CH:5]=[CH:6][CH:7]=1.[Cl-].[O:10]=[C:11]1[N:16]([CH3:17])[C:15](=[O:18])[N:14]([CH3:19])[CH2:13][NH+:12]1[CH3:20].C(=O)(O)[O-].[Na+]>O>[O:10]=[C:11]1[N:16]([CH3:17])[C:15](=[O:18])[N:14]([CH3:19])[CH:13]([C:5]2[CH:6]=[CH:7][C:2]([NH2:1])=[CH:3][C:4]=2[OH:8])[N:12]1[CH3:20]

Participants

5

Reactant 3

HCID 115683-AminophenolHCID 516892Sodium BicarbonateHCID 70575974HCID 70575974, compound

Product 1

HCID 70620130HCID 70620130, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

10.9 (0.1 mol) of m-aminophenol are added to a solution of 19.1 g (0.1 mol) of 2,4-dioxo-1,2,3,4-tetrahydro-1,3,5-trimethyl-s-triazinium chloride in 50 ml of water and the mixture is stirred for some minutes until a clear solution has been produced. 8 g of sodium bicarbonate are then added. 24 g (85) of the same compound as in Example 5 precipitate.

Workup

  1. customhas been produced

Sources & evidence

ORD record
ord-fc23252787d74775916f19f379de55df
Source dataset
uspto-grants-1978_03
Patent number
US04080502

Reaction notes

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