Chloride → HCID 70575974, compound

HRID 1679494Notes

Reaction equation

HRID 1679494 reaction equation
[O:1]=[C:2]1[N:7]([CH3:8])[C:6](=[O:9])[N:5]([CH3:10])[CH2:4][N:3]1[CH3:11].[Cl-:12]>O>[Cl-:12].[O:1]=[C:2]1[N:7]([CH3:8])[C:6](=[O:9])[N:5]([CH3:10])[CH2:4][NH+:3]1[CH3:11]

Participants

4

Reactant 2

HCID 312ChlorideHCID 1816881,3,5-Triazinane-2,4-dione, 1,3,5-trimethyl-

Product 1

HCID 70575974HCID 70575974, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

15.7 g (0.1 mol) of 2,4-dioxo-hexahydro-1,3,5-trimethyl-s-triazine are dissolved in 50 ml of water. 7 g (0.1 mol) of chloride are slowly passed into this solution. The temperature is kept at 25 -30° C by occassional cooling. The aqueous solution is then evaporated in vacuo, and 18 g (94%) of 2,4-dioxo-1,2,3,4-tetrahydro--1,3,5-s-triazinium chloride are thereby obtained as white crystals, which are strongly hygroscopic.

Workup

  1. customis kept at 25 -30° C by occassional cooling
  2. customThe aqueous solution is then evaporated in vacuo, and 18 g (94%) of 2,4-dioxo-1,2,3,4-tetrahydro--1,3,5-s-triazinium chloride
  3. customare thereby obtained as white crystals, which

Sources & evidence

ORD record
ord-14998124f4fd40a5a441a0bbfce67ccd
Source dataset
uspto-grants-1978_03
Patent number
US04080502

Reaction notes

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