HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 20361443, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Benzenesulfonyl chloride | HCID 7369 | — |
| Reactant | 2-Bromo-N-(3-hydroxyphenyl)acetamide | HCID 12764105 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 20361443 | HCID 20361443 | — |
Reaction Steps
To a mixture of 4.4 g. of benzene sulfonyl chloride and 5.7 g. of 3'-hydroxy bromoacetanilide in 100 ml. of methylene chloride is added dropwise 2.6 g. of triethylamine. The product is recovered by washing with cold water, drying and removal of the solvent. There is obtained 9.0 g. of the title compound, nD30 = 1.5830.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04081474 |
| Source dataset | uspto-grants-1978_03 |
| ORD ID | ord-012a25342ff94fd1b475ac06fd60b738 |
| Source note | uspto-grants-1978_03 |