HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 86735573, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 2-(O-aminooxy)ethylamine dihydrochloride | HCID 14362326 | — |
| Reactant | HCID 70627006 | HCID 70627006 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86735573 | HCID 86735573 | — |
Reaction Steps
A mixture of 6.9 mmol (1.67 g) of 3', 4'-dichloro-4-cyanobutyrophenone (melting point 53°-54° C), 6.9 mmol (1.03 g) of 2-aminooxyethylamine dihydrochloride, 6.9 mmol (0.56ml) of pyridine and 5 ml of absolute ethanol was refluxed for 3.5 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04081552 |
| Source dataset | uspto-grants-1978_03 |
| ORD ID | ord-ebdf1b6059554d28af7a35e2b381254f |
| Source note | uspto-grants-1978_03 |