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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1679783Generated: October 31, 2026

Trifluoroacetic acid → HCID 88813774, compound

https://huagongshe.com/reaction/1679783

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 14158799HCID 14158799—
ProductHCID 88813774HCID 88813774—

Reaction Conditions

Temperature0 °C

Reaction Steps

Boc-Ala-Gly-OMe [10 g, 45 mmoles, described by H. U. Immer et al., Helv. Chim. Acta, 57, 730 (1974)] is dissolved in cold (ice bath) trifluoroacetic acid (100 ml). The solution is stirred for 1 hr at 0° C and the solvent evaporated. The residue is dissolved in methanol, added to diethyl ether and the precipitate collected to yield the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04081530
Source datasetuspto-grants-1978_03
ORD IDord-70b1e0cc27e8411d82ffa2ede26c0f25
Source noteuspto-grants-1978_03