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HRID1679832

反应详情

EQUATION

反应方程式

HRID 1679832 的结构方程式

REACTANTS

反应物

1
结构：COC(=O)[C@H](CC(C)C)NC(=O)[C@H](CC(N)=O)NC(=O)OCc1ccccc1
HCID12814329

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)[C@H](CC(C)C)NC(=O)[C@@H](N)CC(N)=O
HCID57097841

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[C].[Pd]
催化剂HCID178418390

未命名化合物

结构：CC(C)(C)O.O
溶剂HCID71401949

2-Methylpropan-2-ol--water (1/1)

C4H12O2

PROCEDURE

实验过程

A solution of 15.0 g of Z-Asn-Leu-OMe in 400 ml of tertiary butanol+water (9:1) is hydrogenated in the presence of 2 g of palladium carbon (10% Pd). On completion of the hydrogenation the catalyst is suctioned off and the filtrate evaporated at 40° C. The residue is further used as it is.

WORKUP

后处理

  1. customthe filtrate evaporated at 40° C