HuagongsheHuagongshe Chemistry Print Report · For research reference only
Z-Asn-Leu-OMe → H-Asn-Leu-OMe
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Z-Asn-Leu-OMe | HCID 12814329 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | 2-Methylpropan-2-ol--water (1/1) | HCID 71401949 | — |
| Product | H-Asn-Leu-OMe | HCID 57097841 | — |
Reaction Steps
A solution of 15.0 g of Z-Asn-Leu-OMe in 400 ml of tertiary butanol+water (9:1) is hydrogenated in the presence of 2 g of palladium carbon (10% Pd). On completion of the hydrogenation the catalyst is suctioned off and the filtrate evaporated at 40° C. The residue is further used as it is.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04271068 |
| Source dataset | uspto-grants-1981_06 |
| ORD ID | ord-a43bb85f02f44400976a0d9376999311 |
| Source note | uspto-grants-1981_06 |