HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 23459045, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 14762563 | HCID 14762563 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 23459045 | HCID 23459045 | — |
Reaction Steps
With stirring, 35 g (0.1 mole) of benzil-di-(2-chloroethyl)ketal and 52 g (0.6 mole) of morpholine are kept for 6 hours at 110° C. After cooling, the product is taken up in ether. The ether layer is washed with water, dried over Na2SO4 and concentrated. The residual oil is dried in a high vacuum at 50°-60° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04271294 |
| Source dataset | uspto-grants-1981_06 |
| ORD ID | ord-d51f6c29f9e0474199093b04b4563e3e |
| Source note | uspto-grants-1981_06 |