Diethylamine → HCID 23459039, compound

Participants

Reaction Steps

20 g (0.057 mole) of benzil-di-(2-chloroethyl)ketal are stirred with 150 g (2.05 moles) of diethylamine for 24 hours at 140° C. in a pressure autoclave. After cooling, the reaction mixture is taken up in ether and extracted with water. The ether layer is dried over Na2SO4 and concentrated. The residual oil is dried in a high vacuum.

Provenance & Evidence