Piperidine → HCID 23459047, compound

Participants

Reaction Steps

With stirring, 27 g (0.1 mole) of benzoin-2-chloroethyl ether and 68 g (0.8 mole) of piperidine are kept for 6 hours at 110° C. After cooling, the product is taken up in ether and the ether layer is washed with water, dried over Na2SO4 and concentrated. The residual oil is taken up in hexane and the crystals obtained are recrystallised from hexane. Melting point: 53° C.

Provenance & Evidence