HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 23459038, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | HCID 14762563 | HCID 14762563 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 23459038 | HCID 23459038 | — |
Reaction Steps
With stirring, 35 g (0.1 mole) of benzil-di-(2-chloroethyl)ketal and 77 g (0.9 mole) of piperidine are kept for 7 hours at 105° C. After cooling, the reaction mixture is diluted with ether and the piperidine hydrochloride is collected by filtration. The ether is distilled off and the residual oil is dried in a high vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04271294 |
| Source dataset | uspto-grants-1981_06 |
| ORD ID | ord-18c53d81939a4726979fb91588587085 |
| Source note | uspto-grants-1981_06 |