HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 23457236, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 23457191 | HCID 23457191 | — |
| Product | HCID 23457236 | HCID 23457236 | — |
Reaction Steps
28.3 g (0.1 mole) of 4-(2,6-dichloroanilino)-3-thiophenacetonitrile are introduced into 150 ml of concentrated sulfuric acid and stirred for one hour at room temperature. It is poured onto ice, and the precipitate which has formed is filtered off. Recrystallization from ethyl acetate yields 4-(2,6-dichloroanilino)-3-thiophenacetamide (m. 172° to 173°).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04272507 |
| Source dataset | uspto-grants-1981_06 |
| ORD ID | ord-b9379a39fe8b4647abdcb1855130d5cb |
| Source note | uspto-grants-1981_06 |