Potassium Iodide → HCID 70548763, compound

Participants

Reaction Steps

To a solution of 1.00 g (3.91 millimoles) of N-(1-tricyclo[4.3.1.12,5 ]undecyl)-3-chloropropionamide and 0.33 g (3.91 millimoles) of piperidine in 20 ml of diethyl ether was added 6 ml of an aqueous solution containing 0.27 g (3.91 millimoles) of sodium hydrogencarbonate and 0.065 g (0.39 millimole) of potassium iodide, and the mixture was refluxed under stirring for 6 hours. The post treatment was carried out in the same manner as described in Example 1 to obtain 1.00 g (the yield being 75%) of the intended compound having a melting point of 207° to 212° C.

Provenance & Evidence