Potassium Iodide → HCID 70550409, compound

Participants

Reaction Steps

To a solution of 1.50 g (6.2 millimoles) of N-(1-tricyclo[4.3.1.12,5 ]undecyl)-2-chloroacetamide and 0.53 g (6.2 millimoles) of piperidine in 50 ml of ethanol was added 10 ml of an aqueous solution containing 0.52 g (6.2 millimoles) of sodium hydrogencarbonate and 0.10 g (0.62 millimole) of potassium iodide, and the mixture was refluxed, under agitation, for 10 hours. The post treatment was carried out in the same manner as described in section (B) of Example 1 to obtain 1.63 g (the yield being 81%) of the intended compound having a melting point of 174° to 176° C. (recrystallized from methanolacetone).

Provenance & Evidence