HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 70550317, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Phthalimide | HCID 6809 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 57141884 | HCID 57141884 | — |
| Product | HCID 70550317 | HCID 70550317 | 32% |
Reaction Steps
Under the same conditions as described in sections (D) and (E) of Example 8, N-(1-tricyclo[4.3.1.12,5 ]undecyl)-2-chloropropionamide was converted to the phthalimide derivative, the derivative was converted to an amine by 80% hydrazine hydrate and the amine was neutralized by hydrogen chloride gas to obtain viscous N-(1-tricyclo[4.3.1.12,5 ]undecyl)-2-aminopropionamide hydrochloride in a yield of 32%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04272536 |
| Source dataset | uspto-grants-1981_06 |
| ORD ID | ord-c5433e56c36a446a9e10c09e901f9027 |
| Source note | uspto-grants-1981_06 |