HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Isocyanate → HCID 12876307, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | HCID 192046 | HCID 192046 | — |
| Solvent | Cyclohexane | HCID 8078 | — |
| Product | HCID 12876307 | HCID 12876307 | — |
Reaction Steps
10.9 g (0.04 mol) of ethyl 1-methyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole-1-acetate are suspended in 200 ml of cyclohexane. 3 ml (0.04 mol) of methyl isocyanate are added. The mixture is heated under reflux for 1 hour. It is allowed to cool overnight in a refrigerator. The precipitate is filtered off. The product is recrystallised from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04272539 |
| Source dataset | uspto-grants-1981_06 |
| ORD ID | ord-b25d27eba5da4af7927b7ce0206b20c2 |
| Source note | uspto-grants-1981_06 |