HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 12876310, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Methyl 2,3,4,9-tetrahydro-1-methyl-1H-pyrido[3,4-b]indole-1-carboxylate | HCID 149110 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12876310 | HCID 12876310 | — |
Reaction Steps
4.8 g (0.02 mol) of methyl 1-methyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole-1-carboxylate are dissolved in 100 ml of ethanol saturated with methylamine. The solution is left at ambient temperature for 48 hours. The solvent is removed and the residue is then taken up in 20 ml of ethanol. The product is filtered off and washed with ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04272539 |
| Source dataset | uspto-grants-1981_06 |
| ORD ID | ord-06199cb348db45458e575e60b24f2ae9 |
| Source note | uspto-grants-1981_06 |