HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 12898562, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 12898549 | HCID 12898549 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12898562 | HCID 12898562 | — |
Reaction Steps
Combine methyl 2-[4-(hexafluoro-2-hydroxy-2-propyl)-2,6-dimethylphenylthio]acetate with 30 ml ethanol and 5 ml 1.0 N sodium hydroxide. Reflux 4 hours, add 5 ml 1.0 N HCl, and extract with ether. Dry, concentrate and recrystallize from ether-hexane to obtain 2-[4-(hexafluoro-2-hydroxy-2-propyl)-2,6-dimethylphenylthio]acetic acid, m.p. 133°-135° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04272550 |
| Source dataset | uspto-grants-1981_06 |
| ORD ID | ord-2719710cf60647469e54702cc4202616 |
| Source note | uspto-grants-1981_06 |