HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluorobenzaldehyde → HCID 53820628, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluorobenzaldehyde | HCID 68009 | — |
| Reactant | Methyl 5-aminopyridine-2-carboxylate | HCID 12457877 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 53820628 | HCID 53820628 | — |
Reaction Steps
The starting material is prepared as follows: The mixture of 11.25 g of 5-aminopyridine-2-carboxylic acid methyl ester, 10.0 g of m-fluorobenzaldehyde and 50 ml of benzene is refluxed for 22 hours on a water trap. It is evaporated and the residue recrystallized from acetonitrile, to yield the 5-(m-fluorobenzylideneamino)-pyridine-2-carboxylic acid methyl ester, melting at 111°-114°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04273779 |
| Source dataset | uspto-grants-1981_06 |
| ORD ID | ord-f10c7f253ce44564a3d9f9d89673a192 |
| Source note | uspto-grants-1981_06 |