HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 12640192, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 5-{[(4-Fluorophenyl)methyl]amino}pyridine-2-carboxylic acid | HCID 12640191 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 12640192 | HCID 12640192 | — |
Reaction Steps
0.5 g of 5-(p-fluorobenzylamino)-pyridine-2-carboxylic acid are dissolved in 5 ml of warm acetic acid and dry hydrogen chloride is added until the solution is saturated. Thereupon, nitrogen is bubbled into the solution for several minutes, the solid formed is collected and washed with diethyl ether to yield the 5-(p-fluorobenzylamino)-pyridine-2-carboxylic acid hydrochloride melting at 248°-253° with decomposition.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04273779 |
| Source dataset | uspto-grants-1981_06 |
| ORD ID | ord-347ece8527764fbfaf96909b43c334fb |
| Source note | uspto-grants-1981_06 |