Phenylhydrazine → HCID 86737801, compound

HRID 1680469Notes

Reaction equation

HRID 1680469 reaction equation
[CH2:1]([NH:7][C:8]1[CH:13]=[CH:12][C:11]([C:14](=O)[CH3:15])=[CH:10][CH:9]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].[C:17]1([NH:23][NH2:24])[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>C(O)(=O)C.C(O)C.O.C(O)(=O)C>[C:17]1([NH:23][N:24]=[C:14]([C:11]2[CH:12]=[CH:13][C:8]([NH:7][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH3:6])=[CH:9][CH:10]=2)[CH3:15])[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1

Participants

5

Reactant 2

HCID 7516PhenylhydrazineHCID 70988841-[4-(Hexylamino)phenyl]ethanone

Product 1

HCID 86737801HCID 86737801, compound

Reagents, catalysts & solvents 2

HCID 18476134Acetic acid ethanolSolventHCID 21899381Acetic acid--water (1/1)Solvent

Procedure

p-Hexylaminoacetophenone dissolved in ethanol acetic acid is treated with a solution of phenylhydrazine in water-acetic acid. After a short time the phenylhydrazone separates out, and is collected and washed with water.

Workup

  1. customis collected
  2. washwashed with water

Sources & evidence

ORD record
ord-a4b089d958aa43bba1ab096c3446fc1f
Source dataset
uspto-grants-1981_06
Patent number
US04273785

Reaction notes

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