HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86737807, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 14158798 | HCID 14158798 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 86737807 | HCID 86737807 | — |
Reaction Steps
26.0 Grams of methyl Boc-D-alanylglycinate is dissolved in 340 ml of acetic acid, and 170 ml of a 6 N solution of hydrogen chloride in dioxane is added to the solution. The reaction mixture is allowed to stand for ten minutes and then the solvent is removed under vacuum. The residue is triturated with diethyl ether. The resulting white precipitate is filtered and washed with diethyl ether to afford methyl-D-alanylglycinate hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04273704 |
| Source dataset | uspto-grants-1981_06 |
| ORD ID | ord-7e8b1d35c45542e5be8db64067871106 |
| Source note | uspto-grants-1981_06 |