HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 23455318, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | alpha-Bromo-4-chlorophenylacetic acid | HCID 10490868 | — |
| Reactant | HCID 178527796 | HCID 178527796 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 23455318 | HCID 23455318 | 70% |
Reaction Steps
An acetone solution of 10.0 g (0.05 moles) 5-chloro-2-mercaptobenzothiazole and 12.5 g. (0.01 moles) α-bromo-(p-chloro)phenylacetic acid containing 50 ml. glacial acetic acid and 20 ml. acetic anhydride is heated in an open flask. When the solution is concentrated to a small volume, the precipitated solid, weighing 15.1 g. (70% yield) is collected.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04275065 |
| Source dataset | uspto-grants-1981_06 |
| ORD ID | ord-725b6700d45a4eba85fce3ce92551c0c |
| Source note | uspto-grants-1981_06 |