HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 4-(naphthalen-1-yloxy)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 762479 | HCID 762479 | — |
| Catalyst | Iron | HCID 23925 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 4-(naphthalen-1-yloxy)aniline | HCID 819583 | — |
Reaction Steps
A mixture of 1.5 liters of water, 40 ml of glacial acetic acid and 1.0 mol of 4-(α-naphthoxy)-nitrobenzene was heated to boiling while stirring. After the boiling temperature had been reached, 200 g of iron powder were added in small portions. When the addition was finished, it was refluxed for 6 hours, while stirring.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04275077 |
| Source dataset | uspto-grants-1981_06 |
| ORD ID | ord-645f2b93eea24ca7bb3c17dc790bef29 |
| Source note | uspto-grants-1981_06 |