反应详情

A mixture of 1.5 liters of water, 40 ml of glacial acetic acid and 1.0 mol of 4-(α-naphthoxy)-nitrobenzene was heated to boiling while stirring. After the boiling temperature had been reached, 200 g of iron powder were added in small portions. When the addition was finished, it was refluxed for 6 hours, while stirring.

1. temperaturewas heated
2. additionWhen the addition
3. temperatureit was refluxed for 6 hours
4. stirringwhile stirring