Pyrogallol → Bendiocarb phenol

HRID 1680760Notes

Reaction equation

HRID 1680760 reaction equation
[C:1]1([CH:9]=[CH:8][CH:7]=[C:5]([OH:6])[C:3]=1[OH:4])[OH:2].CO[C:12](OC)([CH3:14])[CH3:13]>>[CH3:13][C:12]1([CH3:14])[O:2][C:1]2[CH:9]=[CH:8][CH:7]=[C:5]([OH:6])[C:3]=2[O:4]1

Participants

3

Reactant 2

HCID 1057PyrogallolHCID 64952,2-Dimethoxypropane

Product 1

HCID 62765Bendiocarb phenol

Procedure

The pyrogallol is particularly suitable for reaction with 2,2-dimethoxypropane to form 2,2-dimethyl-4-hydroxy-1,3-benzodioxole, and then reaction of this with methyl isocyanate to produce the pesticide 2,2-dimethyl-1,3-benzodioxol-4-yl methylcarbamate.

Sources & evidence

ORD record
ord-6f70c49accbc42b3aad1ed4e01dd13a3
Source dataset
uspto-grants-1981_06
Patent number
US04275247

Reaction notes

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