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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1680879Generated: October 26, 2026

2-(4-Methoxyphenyl)-1,1-dimethylethylamine → alpha-(alpha,alpha-Dimethyl-4-methoxyphenethylimino)-2-benzyloxyacetophenone

https://huagongshe.com/reaction/1680879

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-(4-Methoxyphenyl)-1,1-dimethylethylamineHCID 91892—
Reactant2-Benzyloxyphenylglyoxal hydrateHCID 20434085—
SolventDimethyl SulfoxideHCID 679—
Productalpha-(alpha,alpha-Dimethyl-4-methoxyphenethylimino)-2-benzyloxyacetophenoneHCID 23454850—

Reaction Conditions

Temperature23 °C

Reaction Steps

1.16 g of 2-benzyloxyphenylglyoxal hydrate are dissolved in one ml of dimethylsulfoxide, and a solution of 0.78 g of α,α-dimethyl-4-methoxyphenethylamine in 1.5 ml of dimethylsulfoxide is added thereto. The mixture is stirred at 23° C. for one hour, whereby a solution of α-(α,α-dimethyl-4-methoxyphenethylimino)-2-benzyloxyacetophenone in dimethylsulfoxide is obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04276304
Source datasetuspto-grants-1981_06
ORD IDord-b559079964734a0f83266a3bc1741736
Source noteuspto-grants-1981_06