HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1680882Generated: October 26, 2026
1-(3,4-Dimethoxyphenyl)-2-methylpropan-2-amine → alpha-(alpha,alpha-Dimethyl-3,4-dimethoxyphenethylimino)-2-benzyloxyacetophenone
https://huagongshe.com/reaction/1680882
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-(3,4-Dimethoxyphenyl)-2-methylpropan-2-amine | HCID 13020633 | — |
| Reactant | 2-Benzyloxyphenylglyoxal hydrate | HCID 20434085 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | alpha-(alpha,alpha-Dimethyl-3,4-dimethoxyphenethylimino)-2-benzyloxyacetophenone | HCID 23454857 | — |
Reaction Steps
570 mg of 2-benzyloxyphenylglyoxal hydrate are dissolved in 0.5 ml of dimethylsulfoxide, and a solution of 450 mg of α,α-dimethyl-3,4-dimethoxyphenethylamine in 0.7 ml of dimethylsufoxide is added thereto. The mixture is stirred at 20° C. for 2 hours, whereby a solution of α-(α,α-dimethyl-3,4-dimethoxyphenethylimino)-2-benzyloxyacetophenone in dimethylsufoxide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04276304 |
|---|
| Source dataset | uspto-grants-1981_06 |
|---|
| ORD ID | ord-4c99a4a36c974b8294afe7535561f1b3 |
|---|
| Source note | uspto-grants-1981_06 |
|---|
