HRID1680885

反应详情

EQUATION

反应方程式

HRID 1680885 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
25 °C

PROCEDURE

实验过程

2 g of 2-n-butoxyphenylglyoxal hydrate are dissolved in 2.5 ml of dimethylsulfoxide, and a solution of 1.83 g of α,α-dimethyl-3,4-dimethoxyphenethylamine in one ml of dimethylsulfoxide is added thereto. The mixture is stirred at 25° C. for 30 minutes, whereby a solution of α-(α,α-dimethyl-3,4-dimethoxyphenethylimino)-2-n-butoxyacetophenone in dimethylsulfoxide is obtained.