HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1680885Generated: October 31, 2026
1-(3,4-Dimethoxyphenyl)-2-methylpropan-2-amine → alpha-(alpha,alpha-Dimethyl-3,4-dimethoxyphenethylimino)-2-n-butoxyacetophenone
https://huagongshe.com/reaction/1680885
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-(3,4-Dimethoxyphenyl)-2-methylpropan-2-amine | HCID 13020633 | — |
| Reactant | 2-n-Butoxyphenylglyoxal hydrate | HCID 20434119 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | alpha-(alpha,alpha-Dimethyl-3,4-dimethoxyphenethylimino)-2-n-butoxyacetophenone | HCID 23454847 | — |
Reaction Steps
2 g of 2-n-butoxyphenylglyoxal hydrate are dissolved in 2.5 ml of dimethylsulfoxide, and a solution of 1.83 g of α,α-dimethyl-3,4-dimethoxyphenethylamine in one ml of dimethylsulfoxide is added thereto. The mixture is stirred at 25° C. for 30 minutes, whereby a solution of α-(α,α-dimethyl-3,4-dimethoxyphenethylimino)-2-n-butoxyacetophenone in dimethylsulfoxide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04276304 |
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| Source dataset | uspto-grants-1981_06 |
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| ORD ID | ord-85486a280b2e43458ee0f16aeb905105 |
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| Source note | uspto-grants-1981_06 |
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