反应详情

温度

23 °C

1.31 g of 2-benzyloxyphenylglyoxal hydrate are dissolved in 3.5 ml of dimethylsulfoxide, and 0.97 g of α,α-dimethyl-3,4-methylenedioxyphenethylamine are added thereto. The mixture is stirred at 23° C. for 45 minutes, whereby a solution of α-(α,α-dimethyl-3,4-methylenedioxyphenethylimino)-2-benzyloxyacetophenone in dimethylsulfoxide is obtained.