HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1680888Generated: October 26, 2026
1-(2H-1,3-Benzodioxol-5-yl)-2-methylpropan-2-amine → alpha-(alpha,alpha-Dimethyl-3,4-methylenedioxyphenethylimino)-2-benzyloxyacetophenone
https://huagongshe.com/reaction/1680888
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-(2H-1,3-Benzodioxol-5-yl)-2-methylpropan-2-amine | HCID 13020598 | — |
| Reactant | 2-Benzyloxyphenylglyoxal hydrate | HCID 20434085 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | alpha-(alpha,alpha-Dimethyl-3,4-methylenedioxyphenethylimino)-2-benzyloxyacetophenone | HCID 86737825 | — |
Reaction Steps
1.31 g of 2-benzyloxyphenylglyoxal hydrate are dissolved in 3.5 ml of dimethylsulfoxide, and 0.97 g of α,α-dimethyl-3,4-methylenedioxyphenethylamine are added thereto. The mixture is stirred at 23° C. for 45 minutes, whereby a solution of α-(α,α-dimethyl-3,4-methylenedioxyphenethylimino)-2-benzyloxyacetophenone in dimethylsulfoxide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04276304 |
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| Source dataset | uspto-grants-1981_06 |
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| ORD ID | ord-eb3c6462d2e84cf6ab70b8af83754cd8 |
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| Source note | uspto-grants-1981_06 |
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