1-(2H-1,3-Benzodioxol-5-yl)-2-methylpropan-2-amine → HCID 86737827, compound

HRID 1680890Notes

Reaction equation

HRID 1680890 reaction equation
O.C(O[C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[C:13]([CH:15]=[O:16])=[O:14])CCC.[CH3:17][C:18]([NH2:30])([CH3:29])[CH2:19][C:20]1[CH:25]=[CH:24][C:23]2[O:26][CH2:27][O:28][C:22]=2[CH:21]=1>CS(C)=O>[CH3:29][C:18]([N:30]=[C:15]([O:16][CH2:12][CH2:7][CH2:8][CH3:9])[C:13]([C:8]1[CH:7]=[CH:12][CH:11]=[CH:10][CH:9]=1)=[O:14])([CH3:17])[CH2:19][C:20]1[CH:25]=[CH:24][C:23]2[O:26][CH2:27][O:28][C:22]=2[CH:21]=1

Participants

4

Reactant 2

HCID 130205981-(2H-1,3-Benzodioxol-5-yl)-2-methylpropan-2-amineHCID 204341192-n-Butoxyphenylglyoxal hydrate

Product 1

HCID 86737827HCID 86737827, compound

Reagents, catalysts & solvents 1

HCID 679Dimethyl SulfoxideSolvent2×

Procedure

A mixture of 700 mg of 2-n-butoxyphenylglyoxal hydrate, 500 mg of α,α-dimethyl-3,4-methylenedioxyphenethylamine and 1.5 ml of dimethylsulfoxide is stirred at room temperature for 45 minutes, whereby a solution of α-(α,α-dimethyl-3,4-methylenedioxyphenethylimino)-2-n-butoxyacetophenone in dimethylsulfoxide is obtained.

Sources & evidence

ORD record
ord-66b8b20a3e8b44d989ff2d91f7c957d3
Source dataset
uspto-grants-1981_06
Patent number
US04276304

Reaction notes

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