HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2H-1,3-Benzodioxol-5-yl)-2-methylpropan-2-amine → HCID 86737827, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2H-1,3-Benzodioxol-5-yl)-2-methylpropan-2-amine | HCID 13020598 | — |
| Reactant | 2-n-Butoxyphenylglyoxal hydrate | HCID 20434119 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 86737827 | HCID 86737827 | — |
Reaction Steps
A mixture of 700 mg of 2-n-butoxyphenylglyoxal hydrate, 500 mg of α,α-dimethyl-3,4-methylenedioxyphenethylamine and 1.5 ml of dimethylsulfoxide is stirred at room temperature for 45 minutes, whereby a solution of α-(α,α-dimethyl-3,4-methylenedioxyphenethylimino)-2-n-butoxyacetophenone in dimethylsulfoxide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04276304 |
| Source dataset | uspto-grants-1981_06 |
| ORD ID | ord-66b8b20a3e8b44d989ff2d91f7c957d3 |
| Source note | uspto-grants-1981_06 |