HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylthiocarbamoyl chloride → HCID 23454946, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylthiocarbamoyl chloride | HCID 27871 | — |
| Reactant | Acetic acid, 2-(4-aminophenyl)hydrazide | HCID 81068 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 23454953 | HCID 23454953 | — |
| Product | HCID 23454946 | HCID 23454946 | — |
Reaction Steps
The procedure for the preparation of NA-1 in Example 1 was followed with 1-acetyl-2-(4-aminophenyl)hydrazine (0.82 g, 0.005 mole), dimethylthiocarbamoyl chloride (0.62 g, 0.005 mole) and N,N-diisopropylethylamine (0.65 g, 0.005 mole). Yield 0.30 g (24 percent), m.p. 187°-189° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04276364 |
| Source dataset | uspto-grants-1981_06 |
| ORD ID | ord-6cdf09f407404029a54d47ab8b1c0579 |
| Source note | uspto-grants-1981_06 |