Dibenzylamine → HCID 23454959, compound

HRID 1680897Notes

Reaction equation

HRID 1680897 reaction equation
[CH2:1]([NH:8][CH2:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:16]([NH:19][NH:20][C:21]1[CH:26]=[CH:25][C:24]([N:27]=[C:28]=[S:29])=[CH:23][CH:22]=1)(=[O:18])[CH3:17].C(NNC1C=CC(NC(N(CC2C=CC=CC=2)CC2C=CC=CC=2)=S)=CC=1)=O>>[C:16]([NH:19][NH:20][C:21]1[CH:26]=[CH:25][C:24]([NH:27][C:28]([N:8]([CH2:1][C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)[CH2:9][C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)=[S:29])=[CH:23][CH:22]=1)(=[O:18])[CH3:17]

Participants

4

Reactant 3

HCID 7656DibenzylamineHCID 20454059HCID 20454059, compoundHCID 23454956HCID 23454956, compound

Product 1

HCID 23454959HCID 23454959, compound

Procedure

Dibenzylamine (0.20 g, 0.001 mole) and 4-(2-acetylhydrazino)phenyl isothiocyanate (0.21 g, 0.001 mole) were reacted according to the procedure described for NA-11 in Example 3. Yield 0.35 g (88 percent), m.p. 207°-209° C.

Sources & evidence

ORD record
ord-57ded5c1ea7e438eae4f2dd3ce10c447
Source dataset
uspto-grants-1981_06
Patent number
US04276364

Reaction notes

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