Pyrrolidine → HCID 23454971, compound

HRID 1680902Notes

Reaction equation

HRID 1680902 reaction equation
N1CCCC1.C(NNC1(N=C=S)C=CC=CC1)=O.[CH:19]([NH:21][NH:22][C:23]1[CH:28]=[CH:27][C:26]([NH:29][C:30]([N:32]([CH2:40][C:41]2[CH:46]=[CH:45]C=CC=2)CC2C=CC=CC=2)=[S:31])=[CH:25][CH:24]=1)=[O:20]>>[CH:19]([NH:21][NH:22][C:23]1[CH:24]=[CH:25][C:26]([NH:29][C:30]([N:32]2[CH2:40][CH2:41][CH2:46][CH2:45]2)=[S:31])=[CH:27][CH:28]=1)=[O:20]

Participants

4

Reactant 3

HCID 31268PyrrolidineHCID 23454956HCID 23454956, compoundHCID 23454969HCID 23454969, compound

Product 1

HCID 23454971HCID 23454971, compound

Procedure

Pyrrolidine (0.071 g, 0.001 mole) and 1-(2-formylhydrazino)phenyl isothiocyanate (0.19 g, 0.001 mole) were reacted according to the procedure described for NA-11 in Example 3. Yield 0.15 g (58 percent), m.p. 199°-201° C.

Sources & evidence

ORD record
ord-9efc38b06dfd4dd18f52ba090da51e72
Source dataset
uspto-grants-1981_06
Patent number
US04276364

Reaction notes

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