Ethanol → Ethyl N-phenylcarbamate

HRID 1680948Notes

Reaction equation

HRID 1680948 reaction equation
C1(N[C:8]([NH:10][C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[O:9])C=CC=CC=1.[CH2:17]([OH:19])[CH3:18]>>[CH3:18][CH2:17][O:19][C:8]([NH:10][C:11]1[CH:12]=[CH:13][CH:14]=[CH:15][CH:16]=1)=[O:9]

Participants

3

Reactant 2

HCID 702EthanolHCID 7595Carbanilide

Product 1

HCID 7591Ethyl N-phenylcarbamateYield 93%

Procedure

Following the same procedures as in Example 8, a total amount of N,N'-diphenyl urea crystal was reacted with 50.00 g of ethyl alcohol. After the reaction, the reaction mixture was analyzed to obtain a 93% yield for N-phenylethyl carbamate and a 95% yield for aniline.

Workup

  1. customAfter the reaction

Sources & evidence

ORD record
ord-ef3c15c74cde4816b3781748b5bdecde
Source dataset
uspto-grants-1992_12
Patent number
USRE034137

Reaction notes

Loading…