1,2-Dichloro-4-nitrobenzene → HCID 19807715, compound

HRID 1680949Notes

Reaction equation

HRID 1680949 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([N+:9]([O-:11])=[O:10])[CH:5]=[CH:6][C:7]=1Cl.[CH3:12][O:13][CH2:14][CH2:15][NH2:16]>>[CH3:12][O:13][CH2:14][CH2:15][NH:16][C:7]1[CH:6]=[CH:5][C:4]([N+:9]([O-:11])=[O:10])=[CH:3][C:2]=1[Cl:1]

Participants

3

Reactant 2

HCID 74431,2-Dichloro-4-nitrobenzeneHCID 80182-Methoxyethylamine

Product 1

HCID 19807715HCID 19807715, compound

Procedure

0.3 mol (56.2 g) of 3,4-dichloronitrobenzene in 170 ml of 2-methoxyethylamine is heated to reflux for 3 hours.

Workup

  1. temperatureto reflux for 3 hours

Sources & evidence

ORD record
ord-a64e02f7b3b84a9289dfb9c8f115be35
Source dataset
uspto-grants-1992_12
Patent number
US05167669

Reaction notes

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