HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyethylamine → HCID 19807716, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyethylamine | HCID 8018 | — |
| Reactant | 2-Chloro-5-nitroanisole | HCID 70519 | — |
| Product | HCID 19807716 | HCID 19807716 | — |
Reaction Steps
0.3 mol (56.2 g) of 4-chloro-3-methoxynitrobenzene in 170 ml of 2-methoxyethylamine is heated to reflux for 18 hours. The excess 2-methoxyethylamine is distilled off. The reaction medium is diluted with 300 g of ice-cold water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05167669 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-fd955764502a44eabc040b9209f61150 |
| Source note | uspto-grants-1992_12 |