2-Methoxyethylamine → HCID 19807716, compound

HRID 1680950Notes

Reaction equation

HRID 1680950 reaction equation
Cl[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][C:3]=1[O:11][CH3:12].[CH3:13][O:14][CH2:15][CH2:16][NH2:17]>>[CH3:13][O:14][CH2:15][CH2:16][NH:17][C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][C:3]=1[O:11][CH3:12]

Participants

3

Reactant 2

HCID 80182-MethoxyethylamineHCID 705192-Chloro-5-nitroanisole

Product 1

HCID 19807716HCID 19807716, compound

Procedure

0.3 mol (56.2 g) of 4-chloro-3-methoxynitrobenzene in 170 ml of 2-methoxyethylamine is heated to reflux for 18 hours. The excess 2-methoxyethylamine is distilled off. The reaction medium is diluted with 300 g of ice-cold water.

Workup

  1. temperatureto reflux for 18 hours
  2. distillationThe excess 2-methoxyethylamine is distilled off
  3. additionThe reaction medium is diluted with 300 g of ice-cold water

Sources & evidence

ORD record
ord-fd955764502a44eabc040b9209f61150
Source dataset
uspto-grants-1992_12
Patent number
US05167669

Reaction notes

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