HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl orthoacetate → HCID 14802298, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl orthoacetate | HCID 66221 | — |
| Reactant | HCID 15023099 | HCID 15023099 | — |
| Product | HCID 14802298 | HCID 14802298 | — |
Reaction Steps
14 g (64 mmol) of 8-amino-3-chloro-7-ethylaminoquinoline and 42 g (0.26 mol) of triethyl orthoacetate are stirred at 100° C. for 1 hour. The mixture is allowed to cool to room temperature, excess orthoester is evaporated off, and the residue is recrystallized from ethyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05167695 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-760d525b50e44d8493931c58cb8d965b |
| Source note | uspto-grants-1992_12 |