Sodium Hydroxide → HCID 131717657, compound

HRID 1680973Notes

Reaction equation

HRID 1680973 reaction equation
[C:1]([NH:14][CH:15]([CH2:19][CH2:20][CH2:21][CH3:22])[C:16]([OH:18])=[O:17])(=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[OH-].[Na+].[Cl-].[Ca+2:26].[Cl-]>O>[Ca+2:26].[C:1]([NH:14][CH:15]([CH2:19][CH2:20][CH2:21][CH3:22])[C:16]([O-:18])=[O:17])(=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[C:1]([NH:14][CH:15]([CH2:19][CH2:20][CH2:21][CH3:22])[C:16]([O-:18])=[O:17])(=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

Participants

5

Reactant 3

HCID 14798Sodium HydroxideHCID 5284359Calcium ChlorideHCID 20064843HCID 20064843, compound

Product 1

HCID 131717657HCID 131717657, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

In a procedure similar to those described in Production Examples 4 and 5, 20 g of N-lauroylaminohexanoic acid, 2.6 g of sodium hydroxide, 180 g of ion exchanged water and 71 g of 10% by weight aqueous solution of calcium chloride were used. Thus, 21.1 g of the target N-lauroylaminohexanoic acid calcium salt was obtained as white crystals (yield: 99.6%).

Sources & evidence

ORD record
ord-c0ac006c1199458a89fffe74394d6f77
Source dataset
uspto-grants-1992_12
Patent number
US05167709

Reaction notes

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