HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10543796, compound → HCID 135493470, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10543796 | HCID 10543796 | — |
| Reactant | N,N-dimethylformamide ethanol | HCID 19794673 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 135493470 | HCID 135493470 | — |
Reaction Steps
Obtained using the procedure described in section b of Example 9, starting with 15.0 g (0.0466 mole) of 4-amino-2-[(3,4-dichlorophenoxy)methyl]pteridine in 1500 ml of 5% aqueous sodium hydroxide. Heating time: 6 hours under reflux. Yld: 10.0 g (66%), m.p. 285°-287° C. (ethanol/N,N-dimethylformamide).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05167949 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-500baee714bb4d25836e300da45b6fcf |
| Source note | uspto-grants-1992_12 |