HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → 5,5-Dimethyl-2-phenyl-1,3-thiazolidine-4-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | L-Penicillamine | HCID 92863 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | 5,5-Dimethyl-2-phenyl-1,3-thiazolidine-4-carboxylic acid | HCID 41947 | — |
Reaction Steps
One mole of benzaldehyde was dissolved in 100 cc of 90% ethanol with continuous stirring. One mole of penicillamine was dissolved in water with continuous stirring. The two solutions were then mixed together while stirring was continued. The solution was left to stand at room temperature. Within 15 minutes, a white precipitate occurred. The white precipitate was washed with distilled water through sintered glass. The washed precipitate was then dryed at 100° C. to obtain crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05169858 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-b4e6c42e1d1f492cb240c1c87439436c |
| Source note | uspto-grants-1992_12 |