Glyceryl Monooleate → Monoolein Taurocholic acid

HRID 1681274Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1681274
[CH3:1][C@@H:2]([C@@H:14]1[C@@:18]2([CH3:35])[C@@H:19]([OH:34])[CH2:20][C@@H:21]3[C@@:26]4([CH3:32])[CH2:27][CH2:28][C@@H:29]([OH:31])[CH2:30][C@H:25]4[CH2:24][C@@H:23]([OH:33])[C@H:22]3[C@@H:17]2[CH2:16][CH2:15]1)[CH2:3][CH2:4][C:5]([NH:7][CH2:8][CH2:9][S:10]([O-:13])(=[O:12])=[O:11])=[O:6].[Na+:36].[CH3:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44]/[CH:45]=[CH:46]\[CH2:47][CH2:48][CH2:49][CH2:50][CH2:51][CH2:52][CH2:53][C:54]([O:56][CH2:57][CH:58]([OH:61])[CH2:59][OH:60])=[O:55]>O>[CH3:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44]/[CH:45]=[CH:46]\[CH2:47][CH2:48][CH2:49][CH2:50][CH2:51][CH2:52][CH2:53][C:54]([O:56][CH2:57][CH:58]([OH:61])[CH2:59][OH:60])=[O:55].[CH3:1][C@@H:2]([C@@H:14]1[C@@:18]2([CH3:35])[C@@H:19]([OH:34])[CH2:20][C@@H:21]3[C@@:26]4([CH3:32])[CH2:27][CH2:28][C@@H:29]([OH:31])[CH2:30][C@H:25]4[CH2:24][C@@H:23]([OH:33])[C@H:22]3[C@@H:17]2[CH2:16][CH2:15]1)[CH2:3][CH2:4][C:5]([NH:7][CH2:8][CH2:9][S:10]([O-:13])(=[O:11])=[O:12])=[O:6].[Na+:36]

Komponenten

4

Edukt 2

HCID 5283468Glyceryl Monooleate2×HCID 23666345Sodium Taurocholate4×

Produkt 1

HCID 131717675Monoolein Taurocholic acid

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

860 mg of taurocholic acid was dissolved in 40 ml of de-ionized water. Then, 570.6 mg of monoolein was slowly added to the taurocholic acid solution using an ice bath on a sonic mixer. The final monolein and taurocholic acid concentration was 40 mM (the molecular weight of taurocholic acid is 537.7 and that of monoolein is 356.5). The mixture was stored at 10° C. until used.

Aufarbeitung

  1. customwas stored at 10° C.

Quellen und Nachweise

ORD-Eintrag
ord-dc5e465f3d5545bab9192dbb8863fe65
Quelldatensatz
uspto-grants-1992_12
Patentnummer
US05169944

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