HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 15067717, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Benzenesulfonamide | HCID 7370 | — |
| Reactant | 2,6,8-trichloro-7-methylpurine | HCID 250897 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 15067717 | HCID 15067717 | — |
Reaction Steps
10.8 g (50.0 mmol) of the sodium salt of benzenesulfonamide was suspended in 100 ml of DMF; at 60° C., 11.9 g (50.0 mmol) of 7-methyl-2,6,8-trichloropurine was added. After 8 hours at 80° C. and cooling to room temperature, H2O/ice was added, the mixture was acidified with 10% strength hydrochloric acid and the precipitate was suction filtered and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05171353 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-3533c7d6fd4c466898e4b4a747be5324 |
| Source note | uspto-grants-1992_12 |