Hydrochloric Acid → HCID 19806562, compound

Participants

Reaction Steps

A mixture of 5-(2-methylimidazol-1-yl)-2-nitrobenzaldehyde diethyacetal (735 mg), conc-HCl (2.0 ml), water (4.0 ml) and isopropyl alcohol (4.0 ml) was heated under stirring for 1 hour and cooled. The mixture was extracted with dichloromethane and the extract was dried with Na2SO4 and filtered. The filtrate was distilled to give 494 mg (88%) of the title compound.

Provenance & Evidence